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Platinum complexes in reversed and normal phase chromatography. Analytical and preparative separation of enantiomeric olefins
Summary
Type:
HPLC
Application #:
105920
Catalog#:
720120.46 - MN HPLC Column, Nucleosil C18, 100A, 5um, 4.6x150mm
Detection:
RI
Conditions:
temperature 22°C
eluent: methanol - water (5:1)
flow rate 0.8μl/min
pressure 97bar
Authors:
Köhler J
Source:
J Chromatogr 255 (1983) 311 - 333
Details
Legend: Fig. 17. B) Separation of diastereomers formed by the reaction of 2-methylidenebicyclo[3.2.0]heptane (20% ee) with complex III, 1, 3, and 5 = impurities, 2. solvent, 4. complex III, 6. 2-methylidene
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